trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate

Base Information

• Chemical Name: trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate
• CAS No.: 917396-02-2
• Molecular Formula: C₁₈H₁₂Cl₄N₄O₂
• Molecular Weight: 458.131

Synonyms:trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate

Chemical Property of trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate

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Technology Process of trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate

There total 1 articles about trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazine (917396-00-0) + bis(trichloromethyl) carbonate (32315-10-9) → 7-(4-chlorophenyl)-8-phenyl-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one (917396-01-1) + trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate (917396-02-2)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

Reference yield:

7-(4-chlorophenyl)-8-phenyl-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one (917396-01-1) + trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate (917396-02-2) + 4-bromomethyltrifluoromethylbenzene (402-49-3) → 2-(4-(trifluoromethyl)benzyl)-7-(4-chlorophenyl)-8-phenyl-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one

Guidance literature:

With potassium carbonate; In acetone; at 20 - 60 ℃; for 24h;

Reference yield:

7-(4-chlorophenyl)-8-phenyl-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one (917396-01-1) + trichloromethyl 2-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazinecarboxylate (917396-02-2) + 5-(4-bromomethyl-phenyl)-isoxazole (169547-50-6) → 2-(4-(isoxazol-5-yl)benzyl)-7-(4-chlorophenyl)-8-phenyl-[1,2,4]triazolo[4,3-c]pyrimidin-3(2H)-one

Guidance literature:

With potassium carbonate; In acetone; at 20 - 60 ℃; for 17h;

upstream raw materials:

1-(6-(4-chlorophenyl)-5-phenylpyrimidin-4-yl)hydrazine

bis(trichloromethyl) carbonate

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