Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

Base Information

Chemical Name:Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH
CAS No.:102410-79-7
Molecular Formula:C₇H₈O₃S*C₃₁H₄₁N₅O₈
Molecular Weight:783.9
Hs Code.:

Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu<sup>t</sup>*TosOH

Synonyms:Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

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Chemical Property of Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

Chemical Property:

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Technology Process of Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

There total 3 articles about Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104-15-4
toluene-4-sulfonic acid

: 102410-77-5
Pic(3-OBzl)-Thr(Z-Phg-)-D-Abu-Pro-OBu^t

: 102410-79-7
Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 10h; Ambient temperature;
DOI:10.1002/jlac.198619860102

Reference yield:

: 5491-18-9,17609-52-8,53990-33-3,60584-76-1
(S)-N-(benzyloxycarbonyl)phenylglycine

: 102410-79-7
Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / PPA, DMAP, NMM / CH₂Cl₂ / 1) 2 h, -15 to -10 deg C, 2) 6 d, -2 deg C

2: 96 percent / H₂ / 5percent Pd/C / methanol / 10 h / Ambient temperature

With 4-methyl-morpholine; dmap; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jlac.198619860102

Reference yield:

: 102410-52-6
Pic(3-OBzl)-Thr-D-Abu-Pro-OBu^t

: 102410-79-7
Pic(3-OH)-Thr(H-Phg-)-D-Abu-Pro-OBu^t*TosOH

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / PPA, DMAP, NMM / CH₂Cl₂ / 1) 2 h, -15 to -10 deg C, 2) 6 d, -2 deg C

2: 96 percent / H₂ / 5percent Pd/C / methanol / 10 h / Ambient temperature

With 4-methyl-morpholine; dmap; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jlac.198619860102