3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Base Information

Chemical Name:3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol
CAS No.:1432064-19-1
Molecular Formula:C₅₈H₇₀O₁₀S
Molecular Weight:959.254
Hs Code.:

Synonyms:3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Suppliers and Price of 3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

There total 4 articles about 3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1209-19-4
3-(4'-butylphenyl)propanoic acid

: 265312-95-6
3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-glycerol

: 1432064-19-1
3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1002/chem.201203296

Reference yield:

: 265312-93-4
1-O-allyl-2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranoside

: 1432064-19-1
3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Guidance literature:: Multi-step reaction with 2 steps

1: AD-mix-α / tert-butyl alcohol; water / 22 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 h / 20 °C

With dmap; AD-mix-α; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201203296

Reference yield:

: 1200-14-2
4-(n-butyl)benzaldehyde

: 1432064-19-1
3-O-(2,3,4-tri-O-benzyl-6-deoxy-6-thioacetyl-α-D-glucopyranosyl)-1,2-di-O-3-(4-butylphenyl)propanoylglycerol

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine; pyridine / 120 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 h / 20 °C

With piperidine; pyridine; dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; 1: |Knoevenagel Condensation;
DOI:10.1002/chem.201203296