1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

Base Information

Chemical Name:1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene
CAS No.:943328-51-6
Molecular Formula:C₃₀H₅₆N₂O₂
Molecular Weight:476.787
Hs Code.:

Synonyms:1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

Chemical Property:

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Technology Process of 1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

There total 4 articles about 1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1,2-bis(2-butyloctyloxy)-4,5-dinitrobenzene

: 943328-51-6
1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

Guidance literature:: With hydrazine hydrate; nickel; In tetrahydrofuran; for 5h; Heating;
DOI:10.1039/b618833h

Reference yield:

: 1,2-bis(2-butyloctyloxy)benzene

: 943328-51-6
1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / HNO₃ / 16 h / 80 °C

2: 81 percent / hydrazine monohydrate / Raney Ni / tetrahydrofuran / 5 h / Heating

With nitric acid; hydrazine hydrate; nickel; In tetrahydrofuran;
DOI:10.1039/b618833h

Reference yield:

: 85531-02-8
5-(bromomethyl)undecane

: 943328-51-6
1,2-bis((2-butyloctyl)oxy)-4,5-diaminobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH; Bu₄NBr / tetrahydrofuran / 1 h / Heating

1.2: 96 percent / tetrahydrofuran / 72 h / Heating

2.1: 84 percent / HNO₃ / 16 h / 80 °C

3.1: 81 percent / hydrazine monohydrate / Raney Ni / tetrahydrofuran / 5 h / Heating

With tetrabutylammomium bromide; nitric acid; sodium hydride; hydrazine hydrate; nickel; In tetrahydrofuran;
DOI:10.1039/b618833h