3-Trimethylsilyloxybenzoyl chloride

Base Information

Chemical Name:3-Trimethylsilyloxybenzoyl chloride
CAS No.:70799-63-2
Molecular Formula:C₁₀H₁₃ClO₂Si
Molecular Weight:228.751
Hs Code.:
DSSTox Substance ID:DTXSID901278041
Nikkaji Number:J680.151J

Synonyms:3-trimethylsilyloxybenzoyl chloride;3-trimethylsiloxybenzoylchloride;SCHEMBL7912420;UGFXBTRMPVVDPP-UHFFFAOYSA-N;DTXSID901278041;3-[(Trimethylsilyl)oxy]benzoyl chloride;70799-63-2

Suppliers and Price of 3-Trimethylsilyloxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-Trimethylsilyloxybenzoyl chloride

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:228.0373339
Heavy Atom Count:14
Complexity:213

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)OC1=CC=CC(=C1)C(=O)Cl

Technology Process of 3-Trimethylsilyloxybenzoyl chloride

There total 3 articles about 3-Trimethylsilyloxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3782-84-1
3-trimethylsiloxybenzoic acid trimethylsilyl ester

: 70799-63-2
3-(trimethylsiloxy)benzoyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; for 3h; Heating;

Reference yield:

: 99-06-9
3-Carboxyphenol

: 70799-63-2
3-(trimethylsiloxy)benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / triethylamine / toluene / 2 h / Heating

2: 75 percent / SOCl₂ / CH₂Cl₂ / 3 h / Heating

With thionyl chloride; triethylamine; In dichloromethane; toluene;

Reference yield:

: 99-06-9
3-Carboxyphenol

: 70799-63-2
3-(trimethylsiloxy)benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 16 h / 60 °C

2: thionyl chloride / acetone / 2 h / 0 °C

With thionyl chloride; triethylamine; In acetone;
DOI:10.1021/acs.jafc.6b03318