C₅₂H₉₀O₈Si₃

Base Information

Chemical Name:C₅₂H₉₀O₈Si₃
CAS No.:1264660-76-5
Molecular Formula:C₅₂H₉₀O₈Si₃
Molecular Weight:927.538
Hs Code.:

C<sub>52</sub>H<sub>90</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₅₂H₉₀O₈Si₃

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Chemical Property of C₅₂H₉₀O₈Si₃

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Technology Process of C₅₂H₉₀O₈Si₃

There total 6 articles about C₅₂H₉₀O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₂H₉₂O₈Si₃

: 1264660-76-5
C₅₂H₉₀O₈Si₃

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 19h; Molecular sieve;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-83-2
C₂₇H₂₇O₇P

: 1264660-76-5
C₅₂H₉₀O₈Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 °C

1.2: 1 h / 50 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

3.2: 2.5 h

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

With 1H-imidazole; tetrapropylammonium perruthennate; dimethylsulfide borane complex; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 1.2: Suzuki-Miyaura coupling;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-88-7
C₄₃H₆₈O₇Si₂

: 1264660-76-5
C₅₂H₉₀O₈Si₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

2.2: 2.5 h

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

With 1H-imidazole; tetrapropylammonium perruthennate; dimethylsulfide borane complex; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol102925d