[({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

Base Information

• Chemical Name: [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester
• CAS No.: 161086-31-3
• Molecular Formula: C₂₅H₃₅N₅O₁₀
• Molecular Weight: 565.58

Synonyms:[({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

Chemical Property of [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

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Technology Process of [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester

There total 6 articles about [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(3aS,4R,6R,6aS)-4-[2-(2-Benzyloxycarbonylamino-acetylamino)-acetylamino]-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methyl ester (161086-30-2) → [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (161086-31-3)

Guidance literature:

With hydrazine hydrate; In methanol;

DOI:10.1016/S0040-4039(00)78525-X

Reference yield:

CbzGlyGly (2566-19-0) → [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (161086-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / dicyclohexylcarbodiimide, 1-hydroxybenztriazole

2: 68 percent / hydrazine hydrate / methanol

With benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol;

DOI:10.1016/S0040-4039(00)78525-X

Reference yield:

(3aS,4S,6R,6aS)-4-Amino-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methyl ester (153796-89-5) → [({[(3aS,4R,6R,6aS)-6-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydrazinocarbonyl-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid benzyl ester (161086-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / dicyclohexylcarbodiimide, 1-hydroxybenztriazole

2: 68 percent / hydrazine hydrate / methanol

With benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In methanol;

DOI:10.1016/S0040-4039(00)78525-X

upstream raw materials:

(3aS,4R,6R,6aS)-4-[2-(2-Benzyloxycarbonylamino-acetylamino)-acetylamino]-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methyl ester

CbzGlyGly

(3aS,4S,6R,6aS)-4-Amino-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methyl ester

(3aS,4R,6R,6aS)-4-Amino-6-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methyl ester

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