(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

Base Information

Chemical Name:(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate
CAS No.:909128-70-7
Molecular Formula:C₁₂H₁₇F₃O₅S
Molecular Weight:330.325
Hs Code.:

Synonyms:(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

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Chemical Property of (R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

Chemical Property:

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Technology Process of (R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

There total 2 articles about (R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 152187-06-9
(R)-5-(tert-butyldimethylsilyloxy)-2-[(trifluoromethanesulfonyl)oxy]-1,3,3-trimethylcyclohex-1-ene

: 909128-70-7
(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: (n-Bu)4NF / tetrahydrofuran / 4 h / 25 °C

2: 0.949 g / pyridine / 13 h / 25 °C

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/jo060490z

Reference yield:

: (4R)-4-hydroxy-2,6,6-trimethylcyclohex-1-enyltrifluoromethanesulfonate

: 108-24-7
acetic anhydride

: 909128-70-7
(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

Guidance literature:: With pyridine; at 25 ℃; for 13h;
DOI:10.1021/jo060490z

Reference yield: 76.0%

: 909128-70-7
(R)-4-acetoxy-2,6,6-trimethylcyclohex-1-en-1-yl trifluoromethanesulfonate

: 6153-06-6,105-29-3
(E)-3-methylpent-2-en-4-yn-1-ol

: 909128-71-8
(1R,3'E)-4-(5-hydroxy-3-methylpent-3-en-1-yn-1-yl)-3,5,5-trimethylcyclohex-3-en-1-yl acetate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 60 ℃; for 6h;
DOI:10.1021/jo060490z