Technology Process of C35H41ClO9
There total 9 articles about C35H41ClO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chlorotriisopropylsilane; boron trifluoride diethyl etherate;
In
acetonitrile;
at 10 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane; acetonitrile / 20 - 50 °C / Cooling
2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 °C
3.1: 12 h / 0 - 20 °C
4.1: N-ethyl-N,N-diisopropylamine; dmap / tetrahydrofuran / 2 h / 0 °C
5.1: chlorotriisopropylsilane; boron trifluoride diethyl etherate / acetonitrile / 10 °C
With
triethylsilane; dmap; n-butyllithium; chlorotriisopropylsilane; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
1.2: 2 h / -78 °C
2.1: 12 h / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine; dmap / tetrahydrofuran / 2 h / 0 °C
4.1: chlorotriisopropylsilane; boron trifluoride diethyl etherate / acetonitrile / 10 °C
With
dmap; n-butyllithium; chlorotriisopropylsilane; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; acetonitrile;
