cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

Base Information

Chemical Name:cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina
CAS No.:78945-80-9
Molecular Formula:C₁₇H₁₂ClNO₂
Molecular Weight:297.741
Hs Code.:

Synonyms:cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

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Chemical Property of cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

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Technology Process of cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

There total 5 articles about cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 78945-82-1
1-metossi-3-carbossi-4-fenilisochinolina

: 78945-80-9
cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

Guidance literature:: With thionyl chloride; at 80 ℃; for 2h;

Reference yield:

: 37617-98-4
4-phenyl-3-isocoumarincarboxylic acid

: 78945-80-9
cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / 25percent NH₃ / ethanol / 48 h / Ambient temperature

2: 81 percent / 10percent H₂SO₄ / 10 h / Heating

3: 92 percent / POCl₃, PCl₅ / 3 h / 140 °C

4: 1.) methanol, reflux, 4 h; 2.) water, reflux, 10 min

5: 94 percent / thionyl chloride / 2 h / 80 °C

With ammonium hydroxide; thionyl chloride; phosphorus pentachloride; sulfuric acid; trichlorophosphate; In ethanol;

Reference yield:

: 69454-47-3
3-carbossimetil-4-fenil-1,2-diidro-1-ossiisochinolina

: 78945-80-9
cloruro acido della 1-metossi-3-carbossi-4-fenilisochinolina

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / POCl₃, PCl₅ / 3 h / 140 °C

2: 1.) methanol, reflux, 4 h; 2.) water, reflux, 10 min

3: 94 percent / thionyl chloride / 2 h / 80 °C

With thionyl chloride; phosphorus pentachloride; trichlorophosphate;