(1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

Base Information

Chemical Name:(1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane
CAS No.:1064077-81-1
Molecular Formula:C₂₀H₃₆BFO₂
Molecular Weight:338.314
Hs Code.:

Synonyms:(1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

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Chemical Property of (1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

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Technology Process of (1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

There total 1 articles about (1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75927-49-0
pinacol vinylboronate

: (E)-2-fluoro-1-dodecen-1-yl(4-methylphenyl)iodonium tetrafluoroborate

: 1064077-81-1
(1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

: 149777-84-4
4,4,5,5-tetramethyl-2-[(E)-2-p-tolylethenyl]-1,3,2-dioxaborolane

: (E)-4-Fluorotetradeca-1,3-diene

Guidance literature:: With tributyl-amine; palladium diacetate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.jfluchem.2007.07.009

Reference yield: 85.0%

: 1064077-81-1
(1E,3E)-2-(4-fluoro-1,3-tetradecadienyl)-4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 1064077-87-7
ethyl 4-{(1E,3E)-4-fluoro-1,3-tetradecadienyl}benzoate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 80 ℃; for 20h;
DOI:10.1016/j.jfluchem.2007.07.009