benzyl 3-bromophenethylcarbamate

Base Information

Chemical Name:benzyl 3-bromophenethylcarbamate
CAS No.:1333145-04-2
Molecular Formula:C₁₆H₁₆BrNO₂
Molecular Weight:334.213
Hs Code.:

Synonyms:benzyl 3-bromophenethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-bromophenethylcarbamate

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Technology Process of benzyl 3-bromophenethylcarbamate

There total 1 articles about benzyl 3-bromophenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58971-11-2
2-(3-bromophenyl)ethanamine

: 501-53-1,94274-21-2
benzyl chloroformate

: 1333145-04-2
benzyl 3-bromophenethylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/jm200980u

Reference yield: 81.0%

: 1333145-04-2
benzyl 3-bromophenethylcarbamate

: 140-88-5,9003-32-1
ethyl acrylate

: 1333145-05-3
(E)-ethyl 3-(3-(2-(((benzyloxy)carbonyl)amino)ethyl)phenyl)acrylate

Guidance literature:: With palladium diacetate; tris-(o-tolyl)phosphine; In acetonitrile; at 160 ℃; for 0.5h; Microwave irradiation;
DOI:10.1021/jm200980u

Reference yield:

: 1333145-04-2
benzyl 3-bromophenethylcarbamate

: 1333145-06-4
ethyl 3-(3-(2-aminoethyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 0.5 h / 160 °C / Microwave irradiation

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; palladium diacetate; tris-(o-tolyl)phosphine; In methanol; acetonitrile;
DOI:10.1021/jm200980u