Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

Base Information

Chemical Name:Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂
CAS No.:90826-11-2
Molecular Formula:C₃₄H₄₈N₆O₁₀
Molecular Weight:700.789
Hs Code.:

Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH<sub>2</sub>

Synonyms:Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

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Chemical Property of Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

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Technology Process of Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

There total 7 articles about Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 96922-23-5
Boc-Leu-Asp-Ser(Bzl)-Tyr-OMe

: 90826-11-2
Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

Guidance literature:: With hydrazine hydrate; In methanol;
DOI:10.1248/cpb.33.184

Reference yield:

: 1080-06-4
L-Tyr-OMe

: 90826-11-2
Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / DCC / dimethylformamide; ethyl acetate / 12 h / Ambient temperature

2: TFA-anisole / 1 h

3: 75 percent / Et₃N / dimethylformamide / 4 h

4: TFA-anisole / 1.) ice bath, 30 min; 2.) 3 h, room temp.

5: 60 percent / Et₃N / dimethylformamide / 4 h

6: 83 percent / hydrazine hydrate (80percent) / methanol

With TFA-anisole; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.184

Reference yield:

: 4218-63-7
N-(4-Methoxybenzyloxycarbonyl)-O-benzyl-L-serine

: 90826-11-2
Boc-Leu-Asp-Ser(Bzl)-Tyr-NHNH₂

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / DCC / dimethylformamide; ethyl acetate / 12 h / Ambient temperature

2: TFA-anisole / 1 h

3: 75 percent / Et₃N / dimethylformamide / 4 h

4: TFA-anisole / 1.) ice bath, 30 min; 2.) 3 h, room temp.

5: 60 percent / Et₃N / dimethylformamide / 4 h

6: 83 percent / hydrazine hydrate (80percent) / methanol

With TFA-anisole; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.184