C₅₂H₇₀O₇

Base Information

Chemical Name:C₅₂H₇₀O₇
CAS No.:1337559-28-0
Molecular Formula:C₅₂H₇₀O₇
Molecular Weight:807.124
Hs Code.:

C<sub>52</sub>H<sub>70</sub>O<sub>7</sub>

Synonyms:C₅₂H₇₀O₇

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Chemical Property of C₅₂H₇₀O₇

Chemical Property:

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Technology Process of C₅₂H₇₀O₇

There total 4 articles about C₅₂H₇₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1337559-27-9
1-deoxy-1-[(4'R,2'E)-4'-hydroxy-2'-octadecenyl]-2,3,4,6-tetra-O-benzyl-α-D-galactopyranose

: 1337559-28-0
C₅₂H₇₀O₇

Guidance literature:: With titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate; In dichloromethane; at -40 - -20 ℃; optical yield given as %de; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo201450s

Reference yield:

: 1233218-77-3
C₂₄H₄₀O₃

: 1337559-28-0
C₅₂H₇₀O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -40 - -20 °C / Inert atmosphere; Molecular sieve

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; n-butyllithium; Cumene hydroperoxide; D-(-)-diisopropyl tartrate; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; 1.2: Wittig methylenation / 4.1: Sharpless asymmetric epoxidation;
DOI:10.1021/jo201450s

Reference yield:

: 1337559-25-7
(R)-1-((heptadec-1-en-3-yloxy)methyl)-4-methoxybenzene

: 1337559-28-0
C₅₂H₇₀O₇

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

3: titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -40 - -20 °C / Inert atmosphere; Molecular sieve

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate; trifluoroacetic acid; In dichloromethane; 3: Sharpless asymmetric epoxidation;
DOI:10.1021/jo201450s