C₆₃H₁₀₂O₁₁Si₄

Base Information

Chemical Name:C₆₃H₁₀₂O₁₁Si₄
CAS No.:945468-45-1
Molecular Formula:C₆₃H₁₀₂O₁₁Si₄
Molecular Weight:1147.84
Hs Code.:

C<sub>63</sub>H<sub>102</sub>O<sub>11</sub>Si<sub>4</sub>

Synonyms:C₆₃H₁₀₂O₁₁Si₄

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Chemical Property of C₆₃H₁₀₂O₁₁Si₄

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Technology Process of C₆₃H₁₀₂O₁₁Si₄

There total 31 articles about C₆₃H₁₀₂O₁₁Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄O₅

: 945468-45-1
C₆₃H₁₀₂O₁₁Si₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

2.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

3.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

4.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

5.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

6.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

7.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

7.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

8.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

9.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

10.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

11.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene; 2.1: Katsuki-Sharpless asymmetric epoxidation / 7.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-62-2
C₁₄H₂₀O₃

: 945468-45-1
C₆₃H₁₀₂O₁₁Si₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: OsO₄; NMO / dioxane / 1 h / 23 °C / pH 7

1.2: 68 percent / NaIO₄ / dioxane / 3 h

2.1: 99 percent / NaH / tetrahydrofuran / 12.5 h / 23 °C

3.1: 73 percent / DIBALH / CH₂Cl₂ / 0.67 h / -78 °C

4.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

5.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

6.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

7.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

8.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

9.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

9.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

10.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

11.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

12.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

13.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; osmium(VIII) oxide; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; benzene; 2.1: Horner-Wadsworth-Emmons reaction / 4.1: Katsuki-Sharpless asymmetric epoxidation / 9.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-63-3
C₁₅H₂₂O₄

: 945468-45-1
C₆₃H₁₀₂O₁₁Si₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: (+)-diisopropyl tartrate; Ti(OiPr)4; TBHP / 4A MS / CH₂Cl₂ / 12 h / -30 °C

2.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1 h / 24 °C

3.1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / -40 °C

4.1: 89 percent / K₂CO₃ / methanol / 0.03 h / 23 °C

5.1: 87 percent / TPAP; NMO; 4A MS / CH₂Cl₂ / 0.5 h / 0 °C

6.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

6.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

7.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

8.1: 93 percent / K₂CO₃ / methanol / 2 h / 24 °C

9.1: 95 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 2 h / 0 °C

10.1: 2,6-lutidine / CH₂Cl₂ / 1 h / -20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; lithium aluminium tetrahydride; N-methyl-2-indolinone; cerium(III) chloride; tetrapropylammonium perruthennate; L-(+)-diisopropyl tartrate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 4A MS; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene; 1.1: Katsuki-Sharpless asymmetric epoxidation / 6.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136