3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

Base Information

Chemical Name:3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol
CAS No.:1196677-74-3
Molecular Formula:C₅₂H₆₂O₁₉
Molecular Weight:991.053
Hs Code.:

Synonyms:3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

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Chemical Property of 3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

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Technology Process of 3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

There total 7 articles about 3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 2,3,4,6-tetra-O-methoxyacetyl-1-O-trichloroacetimidoyl-α-D-mannopyranose

: 170900-81-9
3,4,5,6-tetra-O-benzyl-1-O-p-methoxybenzyl-D-myo-inositol

: 1196677-74-3
3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

: 1190224-21-5
C₅₂H₆₂O₁₉

Guidance literature:: 2,3,4,6-tetra-O-methoxyacetyl-1-O-trichloroacetimidoyl-α-D-mannopyranose; 3,4,5,6-tetra-O-benzyl-1-O-p-methoxybenzyl-D-myo-inositol; In dichloromethane; for 0.666667h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1.08333h;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1196677-74-3
3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

: 1190224-21-5
C₅₂H₆₂O₁₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 18 h / 140 °C / Inert atmosphere

2.1: dichloromethane / 0.67 h / Molecular sieve; Inert atmosphere

2.2: 1.08 h / 0 - 20 °C

With di(n-butyl)tin oxide; In dichloromethane; toluene;

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 1196677-74-3
3,4,5,6-tetra-O-benzyl-1-O-(2,3,4,6-tetramethoxyacetyl-α-D-mannopyranosyl)-D-myo-inositol

: 1190224-21-5
C₅₂H₆₂O₁₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 18 h / 140 °C / Inert atmosphere

2.1: dichloromethane / 0.67 h / Molecular sieve; Inert atmosphere

2.2: 1.08 h / 0 - 20 °C

With di(n-butyl)tin oxide; In dichloromethane; toluene;