N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

Base Information

Chemical Name:N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide
CAS No.:1252643-27-8
Molecular Formula:C₂₆H₃₉F₅N₄O₄S₂
Molecular Weight:630.744
Hs Code.:

Synonyms:N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

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Chemical Property of N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

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Technology Process of N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

There total 2 articles about N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1252643-26-7
tert-butyl {[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamoyl}carbamate

: 1252643-27-8
N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

Guidance literature:: tert-butyl {[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamoyl}carbamate; With hydrogenchloride; In diethyl ether; dichloromethane; ethyl acetate; at 0 - 23 ℃; for 60h;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 1252643-22-3
3-(4-amino-3-methylphenyl)-5,5-dimethyl-1-{9-[(4,4,5,5,5-pentafluoro pentyl)sulphanyl]nonyl}imidazolidine-2,4-dione

: 1252643-27-8
N-[4-(4,4-dimethyl-2,5-dioxo-3-{9-[(4,4,5,5,5-pentafluoropentyl)sulphanyl]nonyl}imidazolidin-1-yl)-2-methylphenyl]sulphamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 °C

2: hydrogenchloride / dichloromethane; ethyl acetate; diethyl ether / 60 h / 0 - 23 °C

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane; ethyl acetate;