Technology Process of C17H20O2
There total 5 articles about C17H20O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[Rh(SIMes)(cod)]ClO4; silver perchlorate;
In
cis-1,2-Dichloroethylene;
at 20 ℃;
for 2h;
DOI:10.1002/anie.201206508
- Guidance literature:
-
Multi-step reaction with 2 steps
1: C9H16O4*ClH / dichloromethane / 12 h / 0 - 20 °C
2: [Rh(SIMes)(cod)]ClO4; silver perchlorate / cis-1,2-Dichloroethylene / 2 h / 20 °C
With
C9H16O4*ClH; [Rh(SIMes)(cod)]ClO4; silver perchlorate;
In
cis-1,2-Dichloroethylene; dichloromethane;
DOI:10.1002/anie.201206508
- Guidance literature:
-
Multi-step reaction with 6 steps
1: propionic acid / 23 h / 110 °C
2: lithium aluminium tetrahydride / diethyl ether / 0.33 h / -78 °C
3: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2.5 h / 0 °C
4: p-toluenesulfonic acid monohydrate / methanol / 4 h / 0 - 20 °C
5: C9H16O4*ClH / dichloromethane / 12 h / 0 - 20 °C
6: [Rh(SIMes)(cod)]ClO4; silver perchlorate / cis-1,2-Dichloroethylene / 2 h / 20 °C
With
lithium aluminium tetrahydride; C9H16O4*ClH; [Rh(SIMes)(cod)]ClO4; p-toluenesulfonic acid monohydrate; silver perchlorate; sodium hydride; propionic acid;
In
cis-1,2-Dichloroethylene; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201206508