2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

Base Information

Chemical Name:2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid
CAS No.:1373931-83-9
Molecular Formula:C₂₂H₂₃NO₁₁
Molecular Weight:477.425
Hs Code.:

Synonyms:2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

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Chemical Property of 2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

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Technology Process of 2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

There total 5 articles about 2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1373931-81-7
diethyl 2,2'-((4-(1-(4-(t-butyl)phenoxy)-2-(2-ethoxy-2-oxoethoxy)-2-oxoethyl)-5-nitro-1,2-phenylene)bis(oxy))diacetate

: 1373931-83-9
2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran;
DOI:10.1039/c2pp05320a

Reference yield:

: 1373931-79-3
2-(4,5-bis(ethoxycarbonylmethoxy)-2-nitrophenyl)acetic acid ethoxycarbonylmethyl ester

: 1373931-83-9
2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.08 h

1.2: 3 h / Darkness

2.1: hydrogen bromide / dichloromethane; acetic acid / 0.5 h

3.1: caesium carbonate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 20 °C

4.1: water; sodium hydroxide / tetrahydrofuran

With water; hydrogen bromide; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; In tetrahydrofuran; dichloromethane; acetic acid; acetonitrile;
DOI:10.1039/c2pp05320a

Reference yield:

: 1373931-80-6
2-(4,5-bis(ethoxycarbonylmethoxy)-2-nitrophenyl)-2-bromoacetic acid ethoxycarbonylmethyl ester

: 1373931-83-9
2,2'-((4-((4-(t-butyl)phenoxy)(carboxy)methyl)-5-nitro-1,2-phenylene)bis(oxy))diacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / tetrahydrofuran / 0.5 h / 0 °C

1.2: 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran

With water; caesium carbonate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1039/c2pp05320a