C₃₃H₄₁NO₄Si

Base Information

Chemical Name:C₃₃H₄₁NO₄Si
CAS No.:1379449-97-4
Molecular Formula:C₃₃H₄₁NO₄Si
Molecular Weight:543.778
Hs Code.:

C<sub>33</sub>H<sub>41</sub>NO<sub>4</sub>Si

Synonyms:C₃₃H₄₁NO₄Si

Suppliers and Price of C₃₃H₄₁NO₄Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₄₁NO₄Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₄₁NO₄Si

There total 8 articles about C₃₃H₄₁NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1379449-96-3
C₃₈H₄₉NO₆Si

: 1379449-97-4
C₃₃H₄₁NO₄Si

Guidance literature:: With silica gel; at 160 ℃; for 3.5h; neat (no solvent);
DOI:10.1021/ja301326k

Reference yield:

: 1379449-94-1
C₂₁H₃₂N₂O₆

: 1379449-97-4
C₃₃H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

3: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

4: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

5: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 45 °C / Inert atmosphere

7: silica gel / 3.5 h / 160 °C / neat (no solvent)

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; pyridinium chlorochromate; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; 5: Friedel Crafts acylation / 6: Stille coupling;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-84-9
C₂₆H₃₃NO₆

: 1379449-97-4
C₃₃H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

2: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

3: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 45 °C / Inert atmosphere

4: silica gel / 3.5 h / 160 °C / neat (no solvent)

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; pyridinium chlorochromate; In nitromethane; dichloromethane; N,N-dimethyl-formamide; 2: Friedel Crafts acylation / 3: Stille coupling;
DOI:10.1021/ja301326k