1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)

Base Information

Chemical Name:1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)
CAS No.:220280-45-5
Molecular Formula:C₇H₁₄N₂O₂
Molecular Weight:158.2
Hs Code.:
Mol file:220280-45-5.mol

Synonyms:1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)

Suppliers and Price of 1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)

Chemical Property:

PSA：66.56000
LogP:0.05680

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI)

There total 2 articles about 1-Pyrrolidinecarboxaldehyde, 3-amino-4-(hydroxymethyl)-2-methyl-, (2S,3R,4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 220280-42-2
(3aR,3bR,7aR)-Hexahydro-2-oxa-5-thia-3,6a-diaza-cyclopenta[a]pentalen-6-one

: 220280-45-5
3(S)-amino-4(R)-hydroxymethyl-2(S)-methylpyrrolidine 1-carbaldehyde

Guidance literature:: With hydrogen; nickel; In methanol; water; for 24h; under 760 Torr;
DOI:10.1021/jo9815094

Reference yield:

: (R)-3-Allyl-2-oxo-thiazolidine-4-carbaldehyde oxime

: 220280-45-5
3(S)-amino-4(R)-hydroxymethyl-2(S)-methylpyrrolidine 1-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / toluene / 16 h / 165 - 170 °C

2: 39 percent / H₂ / Raney Ni / methanol; H₂O / 24 h / 760 Torr

With hydrogen; nickel; In methanol; water; toluene;
DOI:10.1021/jo9815094