(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

Base Information

Chemical Name:(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate
CAS No.:1370288-88-2
Molecular Formula:C₃₀H₃₂N₂O₇
Molecular Weight:532.593
Hs Code.:

Synonyms:(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

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Chemical Property of (2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

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Technology Process of (2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

There total 3 articles about (2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1370288-86-0
(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-((tert-butyldimethylsilyloxy)methyl)-tetrahydrofuran-3-yl benzyl carbonate

: 1370288-88-2
(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

Guidance literature:: With hydrogenchloride; water; In ethanol; ethyl acetate; at 20 ℃; for 0.5h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1370288-88-2
(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 6 h / 20 °C

2: hydrogenchloride; water / ethyl acetate; ethanol / 0.5 h / 20 °C

With hydrogenchloride; dmap; water; In ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 3-(5-((tert-butyldimethylsilyloxy)methyl)-4-hydroxy-tetrahydrofuran-2-yl)-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-2(3H)-one

: 1370288-88-2
(2R,3S,5R)-5-(2-oxo-6-(4-pentylphenyl)furo[2,3-d]pyrimidin-3(2H)-yl)-2-(hydroxymethyl)-tetrahydrofuran-3-yl benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 6 h / 20 °C

2: hydrogenchloride; water / ethyl acetate; ethanol / 0.5 h / 20 °C

With hydrogenchloride; dmap; water; In ethanol; dichloromethane; ethyl acetate;