C₅₃H₈₁NO₁₇S

Base Information

Chemical Name:C₅₃H₈₁NO₁₇S
CAS No.:1185160-55-7
Molecular Formula:C₅₃H₈₁NO₁₇S
Molecular Weight:1036.29
Hs Code.:

C<sub>53</sub>H<sub>81</sub>NO<sub>17</sub>S

Synonyms:C₅₃H₈₁NO₁₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₈₁NO₁₇S

Chemical Property:

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Technology Process of C₅₃H₈₁NO₁₇S

There total 4 articles about C₅₃H₈₁NO₁₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185160-54-6
C₅₁H₇₉NO₁₆S

: 108-24-7
acetic anhydride

: 1185160-55-7
C₅₃H₈₁NO₁₇S

Guidance literature:: With dmap; In dichloromethane; at 25 - 28 ℃; for 20h;

Reference yield:

: 10,11-didehydro-11-deoxy-6-O-methylerythromycin A,2',4-diacetate-12-(chloroacetate)

: 1185160-55-7
C₅₃H₈₁NO₁₇S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / acetone / 2.5 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 5 °C / Inert atmosphere; Ice cooling

3.1: sodium acetate / methanol; water / 0.17 h / 20 °C

3.2: 2 h / 25 - 30 °C

4.1: dmap / dichloromethane / 20 h / 25 - 28 °C

With dmap; sodium acetate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; mineral oil;

Reference yield:

: 1006612-32-3
C₅₂H₈₁NO₁₆S

: 1185160-55-7
C₅₃H₈₁NO₁₇S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / methanol; water / 0.17 h / 20 °C

1.2: 2 h / 25 - 30 °C

2.1: dmap / dichloromethane / 20 h / 25 - 28 °C

With dmap; sodium acetate; In methanol; dichloromethane; water;