C₂₅H₂₆N₄O₇S

Base Information

Chemical Name:C₂₅H₂₆N₄O₇S
CAS No.:1355685-79-8
Molecular Formula:C₂₅H₂₆N₄O₇S
Molecular Weight:526.57
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>4</sub>O<sub>7</sub>S

Synonyms:C₂₅H₂₆N₄O₇S

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Chemical Property of C₂₅H₂₆N₄O₇S

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Technology Process of C₂₅H₂₆N₄O₇S

There total 4 articles about C₂₅H₂₆N₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5847-59-6
2-bromo-4-nitrophenol

: 1355685-79-8
C₂₅H₂₆N₄O₇S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

1.2: 24 h / 20 °C

2.1: XPhos; palladium diacetate; sodium t-butanolate / N,N-dimethyl-formamide; toluene / 1 h / 100 °C / Microwave irradiation

3.1: hydrogenchloride; 2,6-dimethylpyridine / methanol; 1,4-dioxane / 43 h / 0 - 20 °C

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

4.2: 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; sodium hydride; potassium carbonate; sodium t-butanolate; XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1355680-37-3
C₁₁H₁₁F₃N₂O₆S

: 1355680-34-0
C₂₅H₃₅BN₂O₆S

: 1355685-79-8
C₂₅H₂₆N₄O₇S

Guidance literature:: C₁₁H₁₁F₃N₂O₆S; C₂₅H₃₅BN₂O₆S; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

With trifluoroacetic acid; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 373380-62-2
2-bromo-1-(methoxymethoxy)-4-nitrobenzene

: 1355685-79-8
C₂₅H₂₆N₄O₇S

Guidance literature:: Multi-step reaction with 3 steps

1.1: XPhos; palladium diacetate; sodium t-butanolate / N,N-dimethyl-formamide; toluene / 1 h / 100 °C / Microwave irradiation

2.1: hydrogenchloride; 2,6-dimethylpyridine / methanol; 1,4-dioxane / 43 h / 0 - 20 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

3.2: 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; potassium carbonate; sodium t-butanolate; XPhos; In 1,4-dioxane; methanol; N,N-dimethyl-formamide; toluene;