6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine

Base Information

• Chemical Name: 6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine
• CAS No.: 651734-03-1
• Molecular Formula: C₁₈H₂₄N₄OS
• Molecular Weight: 344.481

Synonyms:6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine

Chemical Property of 6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine

Chemical Property:

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Technology Process of 6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine

There total 2 articles about 6-cyclohexylmethoxy-N²-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-n-butylsulfanyl-4-cyclohexylmethoxypyrimidin-6-ylamine (945618-70-2) → 6-cyclohexylmethoxy-N2-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine (651734-03-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / mCPBA / CH₂Cl₂ / 17 h

2: trifluoroacetic acid / 2,2,2-trifluoro-ethanol / 2 h / Heating

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; 2,2,2-trifluoroethanol;

DOI:10.1039/b703241b

Reference yield:

4-methylsulfanylaniline (104-96-1) + 2-(n-butane-1-sulfonyl)-4-cyclohexylmethoxypyrimidin-6-ylamine (651733-96-9) → 6-cyclohexylmethoxy-N2-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine (651734-03-1)

Guidance literature:

With trifluoroacetic acid; In 2,2,2-trifluoroethanol; Heating;

DOI:10.1016/S0960-894X(03)00651-6

Reference yield:

6-cyclohexylmethoxy-N2-(4-methylsulfanyl-phenyl)-pyrimidine-2,4-diamine (651734-03-1) → 6-cyclohexylmethoxy-N2-(4-methylsulfanyl-phenyl)-5-nitroso-pyrimidine-2,4-diamine

Guidance literature:

With acetic acid; sodium nitrite; at 80 ℃;

DOI:10.1016/S0960-894X(03)00651-6

upstream raw materials:

4-methylsulfanylaniline

2-(n-butane-1-sulfonyl)-4-cyclohexylmethoxypyrimidin-6-ylamine

2-n-butylsulfanyl-4-cyclohexylmethoxypyrimidin-6-ylamine

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