C₂₇H₃₈N₂O₇

Base Information

Chemical Name:C₂₇H₃₈N₂O₇
CAS No.:1515665-58-3
Molecular Formula:C₂₇H₃₈N₂O₇
Molecular Weight:502.608
Hs Code.:

C<sub>27</sub>H<sub>38</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₇H₃₈N₂O₇

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Chemical Property of C₂₇H₃₈N₂O₇

Chemical Property:

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Technology Process of C₂₇H₃₈N₂O₇

There total 18 articles about C₂₇H₃₈N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1514894-35-9
1-((benzyloxy)methyl)-4-(((2R,3R)-3-methyl-3-((R)-3-((2S,5S)-2-methyl-5-(2-((triethylsilyl)oxy)propan-2-yl)tetrahydrofuran-2-yl)-3-((triethylsilyl)oxy)propyl)oxiran-2-yl)methyl)-2-nitro-1H-pyrrole

: 1515665-58-3
C₂₇H₃₈N₂O₇

Guidance literature:: 1-((benzyloxy)methyl)-4-(((2R,3R)-3-methyl-3-((R)-3-((2S,5S)-2-methyl-5-(2-((triethylsilyl)oxy)propan-2-yl)tetrahydrofuran-2-yl)-3-((triethylsilyl)oxy)propyl)oxiran-2-yl)methyl)-2-nitro-1H-pyrrole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;

In toluene;
DOI:10.1021/ol403246j

Reference yield:

: 1514894-18-8
2-(1-((benzyloxy)methyl)-5-nitro-1H-pyrrol-3-yl)acetaldehyde

: 1515665-58-3
C₂₇H₃₈N₂O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C

1.2: -78 - 20 °C

2.1: potassium carbonate; disodium ethylenediaminetetraacetic acid; sodium tetraborate decahydrate; tetra(n-butyl)ammonium hydrogensulfate; Shi's ketone; Oxone / acetonitrile; water / 2 h / 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

3.2: CSA

With Oxone; Shi's ketone; sodium tetraborate decahydrate; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydrogensulfate; sodium hexamethyldisilazane; disodium ethylenediaminetetraacetic acid; potassium carbonate; In tetrahydrofuran; water; acetonitrile; 1.1: |Julia-Kocienski Olefination / 1.2: |Julia-Kocienski Olefination;
DOI:10.1021/ol403246j

Reference yield:

: 1514894-14-4
1-benzyloxymethyl-2-nitro-4-vinylpyrrole

: 1515665-58-3
C₂₇H₃₈N₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / acetonitrile; water / 0.33 h

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C

2.2: -78 - 20 °C

3.1: potassium carbonate; disodium ethylenediaminetetraacetic acid; sodium tetraborate decahydrate; tetra(n-butyl)ammonium hydrogensulfate; Shi's ketone; Oxone / acetonitrile; water / 2 h / 0 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4.2: CSA

With Oxone; Shi's ketone; sodium tetraborate decahydrate; sulfuric acid; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydrogensulfate; sodium hexamethyldisilazane; disodium ethylenediaminetetraacetic acid; potassium carbonate; In tetrahydrofuran; water; acetonitrile; 2.1: |Julia-Kocienski Olefination / 2.2: |Julia-Kocienski Olefination;
DOI:10.1021/ol403246j