3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

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Chemical Name:3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione
CAS No.:1283089-08-6
Molecular Formula:C₂₂H₂₂N₄O₄
Molecular Weight:406.441
Hs Code.:

Synonyms:3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

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Chemical Property of 3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

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Technology Process of 3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

There total 4 articles about 3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-89-4
piperidine

: C₁₇H₁₂BrN₃O₄

: 1283089-08-6
3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Microwave irradiation;
DOI:10.1021/jo1025805

Reference yield:

: 65833-16-1
3,4-dibromo-1-(4-nitrophenyl)-1H-pyrrole-2,5-dione

: 1283089-08-6
3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 0.05 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 0.5 h / 50 °C / Microwave irradiation

With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jo1025805

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1283089-08-6
3-(N-methyl-N-phenylamino)-1-(4-nitrophenyl)-4-(piperidin-1-yl)-1H-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 8 h / Reflux

2: triethylamine / N,N-dimethyl-formamide / 0.05 h / 20 °C

3: triethylamine / N,N-dimethyl-formamide / 0.5 h / 50 °C / Microwave irradiation

With acetic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jo1025805