N,N-DIMETHYLOXAMICACID

Base Information

• Chemical Name: N,N-DIMETHYLOXAMICACID
• CAS No.: 32833-96-8
• Molecular Formula: C4H7NO3
• Molecular Weight: 117.104
• Hs Code.: 2924199090
• European Community (EC) Number: 674-326-2
• DSSTox Substance ID: DTXSID40375466
• Nikkaji Number: J829.044J
• Wikidata: Q72471091
• Mol file: 32833-96-8.mol

Synonyms:N,N-Dimethyloxamic acid;Aceticacid, (dimethylamino)oxo- (9CI);2-(Dimethylamino)-2-(oxo)acetic acid;(Dimethylamino)(oxo)acetic acid;Oxamic acid, dimethyl- (6CI,8CI);

Chemical Property of N,N-DIMETHYLOXAMICACID

Chemical Property:

• Vapor Pressure: 0.0748mmHg at 25°C
• Melting Point: 114-118 °C
• Refractive Index: 1.465
• Boiling Point: 210.8 °C at 760 mmHg
• PKA: 3.13±0.40(Predicted)
• Flash Point: 81.3 °C
• PSA: 57.61000
• Density: 1.251 g/cm³
• LogP: -0.84080
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: soluble in Methanol
• XLogP3: -0.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 117.042593085
• Heavy Atom Count: 8
• Complexity: 119

Purity/Quality:

97% ^*data from raw suppliers

N,N-Dimethyloxamic Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(=O)C(=O)O

Technology Process of N,N-DIMETHYLOXAMICACID

There total 4 articles about N,N-DIMETHYLOXAMICACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-(dimethylamino)-2-oxoacetate (59571-38-9) → N,N-dimethyloxamic acid (32833-96-8)

Guidance literature:

With potassium hydroxide; In methanol; for 30h;

Reference yield:

→ N,N-dimethyloxamic acid (32833-96-8)

Guidance literature:

With barium dihydroxide;

Reference yield:

N,N-dimethyl-3,3,3-trichloropyruvamide (33064-46-9) → N,N-dimethyloxamic acid (32833-96-8)

Guidance literature:

With water; sodium hydrogencarbonate;

DOI:10.1007/BF00861484

upstream raw materials:

N,N-dimethyl-3,3,3-trichloropyruvamide

methyl 2-(dimethylamino)-2-oxoacetate

Downstream raw materials:

N,N-dimethyl-formamide

methylammonium carbonate

N,N,N'N'-tetramethyl oxamide

2-(dimethylcarbamoyl)-4-methylquinoline

Refernces