2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

Base Information

Chemical Name:2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene
CAS No.:1352447-95-0
Molecular Formula:C₁₈H₁₇N₅OS
Molecular Weight:351.432
Hs Code.:

Synonyms:2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

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Chemical Property of 2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

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Technology Process of 2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

There total 4 articles about 2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 875629-06-4
2-ethylthio-4-phenyl-1-azetine

: 2-azidobenzohydroximoyl chloride

: 1352447-95-0
2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol202924s

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1352447-95-0
2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 2.17 h / 20 °C / Inert atmosphere

1.2: 1.17 h / Cooling with ice; Inert atmosphere

2.1: Lawessons reagent / tetrahydrofuran / 1.33 h / 20 - 60 °C / Inert atmosphere

3.1: dichloromethane / 2 h / 20 °C / Reflux; Inert atmosphere

4.1: triethylamine / diethyl ether / 20 °C / Inert atmosphere

With Lawessons reagent; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol202924s

Reference yield:

: 5661-55-2
4-phenylazetidin-2-one

: 1352447-95-0
2-(2-azidophenyl)-5-ethylthio-7-phenyl-4,1,3-oxadiazabicyclo[3.2.0]hept-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1: Lawessons reagent / tetrahydrofuran / 1.33 h / 20 - 60 °C / Inert atmosphere

2: dichloromethane / 2 h / 20 °C / Reflux; Inert atmosphere

3: triethylamine / diethyl ether / 20 °C / Inert atmosphere

With Lawessons reagent; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ol202924s