1H,1H-Perfluorononylamine

Base Information

• Chemical Name: 1H,1H-Perfluorononylamine
• CAS No.: 355-47-5
• Molecular Formula: C9H4 F17 N
• Molecular Weight: 449.11
• Hs Code.: 2921199090
• European Community (EC) Number: 625-098-8
• DSSTox Substance ID: DTXSID50379930
• Nikkaji Number: J2.394.972E
• Wikidata: Q81985842
• Mol file: 355-47-5.mol

Synonyms:1H,1H-Perfluorononylamine;355-47-5;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-Heptadecafluorononylamine;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononan-1-amine;SCHEMBL3025512;DTXSID50379930;IHVFAVFXCUPMEN-UHFFFAOYSA-N;MFCD01319146;AKOS016015998;FT-0607857;A822865;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluoro-1-nonanamine;2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-Heptadecafluorononylamine, technical, >=90% (T);2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecakis(fluoranyl)nonan-1-amine

Chemical Property of 1H,1H-Perfluorononylamine

Chemical Property:

• Vapor Pressure: 1.35mmHg at 25°C
• Refractive Index: 1.291
• Boiling Point: 172.2°Cat760mmHg
• PKA: 6.07±0.30(Predicted)
• Flash Point: 68.2°C
• PSA: 26.02000
• Density: 1.64g/cm³
• LogP: 5.65480
• Storage Temp.: 2-8°C
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 7
• Exact Mass: 449.0072279
• Heavy Atom Count: 27
• Complexity: 543

Purity/Quality:

98%,99%, ^*data from raw suppliers

1H,1H-Perfluorononylamine 95% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C,Xi
• Statements: 22-34
• Safety Statements: 26-36/37/39-45

MSDS Files:

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(C(C(C(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)N

Technology Process of 1H,1H-Perfluorononylamine

There total 1 articles about 1H,1H-Perfluorononylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perfluorononanamide (82854-34-0) → 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononylamine (355-47-5)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

Reference yield: 74.0%

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononylamine (355-47-5) + phenyl isothiocyanate (103-72-0) → N-heptadecafluorononyl-N'-phenylthiourea

Guidance literature:

In chloroform; Reflux;

DOI:10.1016/j.tetlet.2015.05.056

Reference yield: 68.0%

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononylamine (355-47-5) + 3-[3,4-di(benzyloxy)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid (59727-98-9) → C37H33F17N2O5

Guidance literature:

3-[3,4-di(benzyloxy)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 0.25h;

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononylamine; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/anie.202100064

upstream raw materials:

perfluorononanamide