(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

Base Information

Chemical Name:(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole
CAS No.:266682-69-3
Molecular Formula:C₂₃H₂₆O₄
Molecular Weight:366.457
Hs Code.:

Synonyms:(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

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Chemical Property of (3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

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Technology Process of (3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

There total 12 articles about (3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 274692-75-0
2,5-di-O-benzyl-1,6-O-isopropylidene-D-allo-inositol 3,4-cyclic sulfate

: 266682-69-3
(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

Guidance literature:: With sodium hydrogen telluride; In pyridine; N,N-dimethyl-formamide; benzene; at 20 ℃; for 0.166667h;
DOI:10.1002/1099-0690(200004)2000:7<1285::AID-EJOC1285>3.0.CO;2-Z

Reference yield: 76.0%

: 1053731-46-6
(3aS,4S,4aR,7aR,8S,8aR)-4,8-Bis-benzyloxy-6,6-dimethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxole-2-thione

: 266682-69-3
(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

Guidance literature:: With triethyl phosphite; at 165 ℃;
DOI:10.1002/1099-0690(200004)2000:7<1285::AID-EJOC1285>3.0.CO;2-Z

Reference yield:

: 266682-66-0
(-)-1,6-dideoxy-2,5-di-O-benzyl-3,4-O-isopropylidene-1,6-thio-D-mannitol-S,S-dioxide

: 266682-69-3
(3aR,4R,7R,7aR)-3a,4,7,7a-tetrahydro-2,2-dimethyl-4,7-bis(phenylmethoxy)-1,3-benzodioxole

Guidance literature:: With potassium hydroxide; In tetrachloromethane; water; tert-butyl alcohol; at 20 ℃; for 1.45h;
DOI:10.1016/S0040-4020(00)00011-9