Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

Base Information

Chemical Name:Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide
CAS No.:78479-30-8
Molecular Formula:C₃₄H₄₉NO₈
Molecular Weight:599.765
Hs Code.:

Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

Synonyms:Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

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Chemical Property of Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

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Technology Process of Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

There total 4 articles about Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78443-16-0
Biphenyl-4-carboxylic acid [(1S,2R,5R,6S,7R,8S,9S,10R,12R,13R,15R,17S)-5-ethyl-6,7,12-trihydroxy-2,6,8,10,12,17-hexamethyl-3-oxo-15-(2,4,6-trimethyl-phenyl)-4,14,16-trioxa-bicyclo[11.3.1]heptadec-9-yl]-amide

: 78479-30-8
Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

Guidance literature:: With silica gel; trifluoroacetic acid; In dichloromethane; water; Yield given; Ambient temperature;
DOI:10.1021/ja00401a051

Reference yield:

: 14002-51-8
4-biphenyl-carboxylic acid chloride

: 78479-30-8
Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

2: NaOH / H₂O; tetrahydrofuran; propan-2-ol / Ambient temperature

3: SiO₂, CF₃COOH / H₂O; CH₂Cl₂ / Ambient temperature

With dmap; sodium hydroxide; silica gel; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/ja00401a051

Reference yield:

: 78443-15-9
(1S,2R,4R,5R,7R,9S,10R,13R,14R,15R,19S,20S)-18-(Biphenyl-4-carbonyl)-13-ethyl-4,14-dihydroxy-2,4,10,14,19,20-hexamethyl-7-(2,4,6-trimethyl-phenyl)-6,8,12,16-tetraoxa-18-aza-tricyclo[13.3.1.1^5,9]icosane-11,17-dione

: 78479-30-8
Biphenyl-4-carboxylic acid ((2R,3S,4R,5S,6S,7R,9R,10R,11S,12S,13R)-2-ethyl-3,4,9,10,12-pentahydroxy-3,5,7,9,11,13-hexamethyl-14-oxo-oxacyclotetradec-6-yl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / H₂O; tetrahydrofuran; propan-2-ol / Ambient temperature

2: SiO₂, CF₃COOH / H₂O; CH₂Cl₂ / Ambient temperature

With sodium hydroxide; silica gel; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/ja00401a051