1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

Base Information

Chemical Name:1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene
CAS No.:1616479-83-4
Molecular Formula:C₁₈H₁₇NO
Molecular Weight:263.339
Hs Code.:

Synonyms:1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

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Chemical Property of 1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

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Technology Process of 1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

There total 8 articles about 1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616480-50-2
4-iodo-1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

: 1616479-83-4
1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol; for 18h; under 760.051 Torr;

Reference yield:

: 4424-20-8
2,3,4,5-tetrahydro-1H-3-benzazepine

: 1616479-83-4
1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; trifluoroacetic acid / 1.25 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; ammonium formate / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

4.1: sulfuric acid; sodium nitrite / water / 1 h / 70 °C

5.1: N-iodo-succinimide; trifluoroacetic acid / chloroform / 0.5 h / 20 °C

6.1: potassium carbonate / acetone / 16 h / 20 °C

7.1: polyphosphoric acid / 0.33 h / 90 °C

8.1: hydrogen; palladium on activated charcoal / ethanol / 18 h / 760.05 Torr

With N-iodo-succinimide; sulfuric acid; palladium 10% on activated carbon; palladium on activated charcoal; hydrogen; ammonium formate; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; acetone;

Reference yield:

: 163068-05-1
3-(trifluoroacetyl)-2,3,4,5-tetrahydro-1H-3-benzazepine-7-amine

: 1616479-83-4
1-phenyl-7,8,9,10-tetrahydro-6H-3-oxa-8-azacyclohepta[e]indene

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; sodium nitrite / water / 1 h / 70 °C

2: N-iodo-succinimide; trifluoroacetic acid / chloroform / 0.5 h / 20 °C

3: potassium carbonate / acetone / 16 h / 20 °C

4: polyphosphoric acid / 0.33 h / 90 °C

5: hydrogen; palladium on activated charcoal / ethanol / 18 h / 760.05 Torr

With N-iodo-succinimide; sulfuric acid; palladium on activated charcoal; hydrogen; potassium carbonate; trifluoroacetic acid; sodium nitrite; In ethanol; chloroform; water; acetone;