p-Menth-2-en-8-ol

Base Information

• Chemical Name: p-Menth-2-en-8-ol
• CAS No.: 19651-06-0
• Molecular Formula: C₁₀H₁₈O
• Molecular Weight: 154.252
• European Community (EC) Number: 831-724-2

Synonyms:p-Menth-2-en-8-ol;SCHEMBL9534440;JQHCVOGXBCGGSQ-UHFFFAOYSA-N;19651-06-0;2-(4-methylcyclohex-2-en-1-yl)propan-2-ol;EN300-6731068

Chemical Property of p-Menth-2-en-8-ol

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 154.135765193
• Heavy Atom Count: 11
• Complexity: 158

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1CCC(C=C1)C(C)(C)O

Technology Process of p-Menth-2-en-8-ol

There total 4 articles about p-Menth-2-en-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C16H32OSi → p-Menth-2-en-8-ol (19651-06-0)

Guidance literature:

With methanol; at 20 ℃; for 5h;

DOI:10.1080/10426507.2019.1576680

Reference yield:

terpineol (98-55-5,2438-12-2) → 2-(4-methylcyclohex-2-enyl)propan-2-ol (19651-06-0,19956-41-3,23727-04-0)

Guidance literature:

Multi-step reaction with 3 steps

1: benzophenone; calcium carbonate / ethyl acetate / 36 h / 39 °C / Inert atmosphere; Irradiation

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: triethylamine / toluene / 56 h / Reflux

With benzophenone; triethylamine; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; In dichloromethane; ethyl acetate; toluene;

DOI:10.1021/ol4018744

Reference yield:

(±)-2-(3-(4-chlorophenylthio)-4-methylcyclohexyl)propan-2-ol → 2-(4-methylcyclohex-2-enyl)propan-2-ol (19651-06-0,19956-41-3,23727-04-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: triethylamine / toluene / 56 h / Reflux

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;

DOI:10.1021/ol4018744

upstream raw materials:

terpineol

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