C₅₉H₆₄O₇

Base Information

Chemical Name:C₅₉H₆₄O₇
CAS No.:1388153-43-2
Molecular Formula:C₅₉H₆₄O₇
Molecular Weight:885.153
Hs Code.:

C<sub>59</sub>H<sub>64</sub>O<sub>7</sub>

Synonyms:C₅₉H₆₄O₇

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Chemical Property of C₅₉H₆₄O₇

Chemical Property:

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Technology Process of C₅₉H₆₄O₇

There total 31 articles about C₅₉H₆₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1388153-41-0
C₂₆H₄₀O₇

: 939-26-4
2-bromomethylnaphthyl bromide

: 1388153-43-2
C₅₉H₆₄O₇

Guidance literature:: C₂₆H₄₀O₇; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.5h;

2-bromomethylnaphthyl bromide; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-39-6
C₃₂H₄₄O₄Si

: 1388153-43-2
C₅₉H₆₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

2.1: tert.-butyl lithium; 9-methoxy-9-BBN / diethyl ether; hexane; pentane / 1.08 h / -78 - 20 °C / Inert atmosphere

2.2: 2 h / 50 °C / Inert atmosphere

3.1: Allyl ether; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 - 20 °C / pH 7 / aq. phosphate buffer

4.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 - 20 °C

5.1: 2,2'-azobis(isobutyronitrile); triphenylstannane / toluene / 0.5 h / 110 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 0 - 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

7.2: 0 - 20 °C

With 1H-imidazole; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); Allyl ether; triphenylstannane; tetrabutyl ammonium fluoride; iodine; tert.-butyl lithium; sodium hydride; 9-methoxy-9-BBN; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; pentane; 2.1: Suzuki-Miyaura coupling / 2.2: Suzuki-Miyaura coupling;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-99-5
C₄₈H₇₂O₇Si₂

: 1388153-43-2
C₅₉H₆₄O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 - 20 °C

2.1: 2,2'-azobis(isobutyronitrile); triphenylstannane / toluene / 0.5 h / 110 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

4.2: 0 - 20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); triphenylstannane; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;
DOI:10.1021/ja305864z