C₂₂H₂₃N₇O₃

Base Information

Chemical Name:C₂₂H₂₃N₇O₃
CAS No.:1197338-11-6
Molecular Formula:C₂₂H₂₃N₇O₃
Molecular Weight:433.47
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₃N₇O₃

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Chemical Property of C₂₂H₂₃N₇O₃

Chemical Property:

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Technology Process of C₂₂H₂₃N₇O₃

There total 8 articles about C₂₂H₂₃N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1197338-10-5
C₁₉H₁₈N₆O₂

: 109-90-0
ethyl isocyanate

: 1197338-11-6
C₂₂H₂₃N₇O₃

Guidance literature:: With pyridine; at 20 ℃; for 3h;

Reference yield:

: 1197340-13-8
C₁₉H₂₈N₂O₄Si

: 1197338-11-6
C₂₂H₂₃N₇O₃

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine; HATU / N,N-dimethyl-formamide / 48 h / 20 °C

2: acetic acid / 5 h / 140 °C

3: boron tribromide / dichloromethane / 5 h / 0 - 20 °C

4: sodium azide / dimethyl sulfoxide / 10 h / 70 °C

5: trimethylphosphane / tetrahydrofuran; water; ethyl acetate / 20 °C

6: pyridine / 3 h / 20 °C

With pyridine; sodium azide; boron tribromide; acetic acid; triethylamine; HATU; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1197340-10-5
C₂₀H₃₀N₂O₄Si

: 1197338-11-6
C₂₂H₂₃N₇O₃

Guidance literature:: Multi-step reaction with 7 steps

1: water; lithium hydroxide / methanol / 2 h / Reflux

2: triethylamine; HATU / N,N-dimethyl-formamide / 48 h / 20 °C

3: acetic acid / 5 h / 140 °C

4: boron tribromide / dichloromethane / 5 h / 0 - 20 °C

5: sodium azide / dimethyl sulfoxide / 10 h / 70 °C

6: trimethylphosphane / tetrahydrofuran; water; ethyl acetate / 20 °C

7: pyridine / 3 h / 20 °C

With pyridine; sodium azide; water; boron tribromide; acetic acid; triethylamine; HATU; lithium hydroxide; trimethylphosphane; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;