Technology Process of C32H35F3N2O7
There total 13 articles about C32H35F3N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1002/chem.201003489
- Guidance literature:
-
Multi-step reaction with 7 steps
1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 2.5 h / 20 °C / Inert atmosphere
4: sodium cyanoborohydride / methanol; chloroform-d1 / 5 h / Molecular sieve; Inert atmosphere
5: pyridine / 5 h / 20 - 50 °C / Inert atmosphere
6: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 5 h / 5 °C / Inert atmosphere
7: Dess-Martin periodane / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
pyridine; tetrabutyl ammonium fluoride; sodium cyanoborohydride; caesium carbonate; Dess-Martin periodane; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; methanol; chloroform-d1; dichloromethane; water; N,N-dimethyl-formamide;
3: Dess-Martin oxidation / 7: Dess-Martin oxidation;
DOI:10.1002/chem.201003489
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 5 h / 5 °C / Inert atmosphere
2: Dess-Martin periodane / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
2: Dess-Martin oxidation;
DOI:10.1002/chem.201003489
