N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

Base Information

Chemical Name:N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene
CAS No.:97632-01-4
Molecular Formula:C₂₃H₁₈N₂O₂
Molecular Weight:354.408
Hs Code.:

Synonyms:N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

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Technology Process of N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

There total 2 articles about N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 102-92-1,17082-09-6
cinnamoyl chloride

: 18969-92-1
1-methylaceperimidylene

: 97632-01-4
N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

Guidance literature:: With water; triethylamine; In diethyl ether; for 0.416667h; Heating;
DOI:10.1007/BF00506673

Reference yield:

: 1-methylaceperimidine

: 97632-01-4
N-methyl-N-formyl-N'-cinnamoyl-5,6-diaminoacenaphthylene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / activated manganese dioxide / benzene / 2 h / Heating

2: 93 percent / triethylamine, H₂O / diethyl ether / 0.42 h / Heating

With manganese(IV) oxide; water; triethylamine; In diethyl ether; benzene;
DOI:10.1007/BF00506673