C₁₅H₁₆O₄S

Base Information

Chemical Name:C₁₅H₁₆O₄S
CAS No.:1407512-45-1
Molecular Formula:C₁₅H₁₆O₄S
Molecular Weight:292.356
Hs Code.:

C<sub>15</sub>H<sub>16</sub>O<sub>4</sub>S

Synonyms:C₁₅H₁₆O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₆O₄S

Chemical Property:

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Technology Process of C₁₅H₁₆O₄S

There total 4 articles about C₁₅H₁₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1407512-44-0
C₂₀H₂₅NO₆S

: 1407512-45-1
C₁₅H₁₆O₄S

Guidance literature:: With molybdenum hexacarbonyl; In water; acetonitrile; at 80 ℃; for 20h;
DOI:10.1021/ja309311z

Reference yield:

: 118-72-9
2,6-dimethylbenzene-1-thiol

: 1407512-45-1
C₁₅H₁₆O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 24 h / Inert atmosphere; Reflux

2: magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

3: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); copper(II) bis(trifluoromethanesulfonate); manganese(IV) oxide / chloroform / 24 h / 20 °C / Inert atmosphere

4: molybdenum hexacarbonyl / acetonitrile; water / 20 h / 80 °C

With manganese(IV) oxide; copper(II) bis(trifluoromethanesulfonate); magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); molybdenum hexacarbonyl; In dichloromethane; chloroform; water; acetonitrile;
DOI:10.1021/ja309311z

Reference yield:

: 1407512-39-3
C₁₂H₁₂N₂OS

: 1407512-45-1
C₁₅H₁₆O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

2: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); copper(II) bis(trifluoromethanesulfonate); manganese(IV) oxide / chloroform / 24 h / 20 °C / Inert atmosphere

3: molybdenum hexacarbonyl / acetonitrile; water / 20 h / 80 °C

With manganese(IV) oxide; copper(II) bis(trifluoromethanesulfonate); magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); molybdenum hexacarbonyl; In dichloromethane; chloroform; water; acetonitrile;
DOI:10.1021/ja309311z