N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

Base Information

Chemical Name:N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine
CAS No.:1457967-15-5
Molecular Formula:C₂₆H₃₂N₄O₂
Molecular Weight:432.566
Hs Code.:

N<SUP>4</SUP>-benzyl-3-nitro-6-phenyl-N<SUP>2</SUP>-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

Synonyms:N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

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Chemical Property of N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

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Technology Process of N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

There total 3 articles about N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1457966-69-6
N⁴-benzyl-6-chloro-3-nitro-N²-(2,4,4-trimethylpentan-2-yl)pyridine-2,4-diamine

: 98-80-6
phenylboronic acid

: 1457967-15-5
N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 90 ℃; for 18h; Inert atmosphere; Sealed tube;
DOI:10.1039/c3ob40816g

Reference yield: 57.0%

: 1457967-15-5
N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 90 ℃; for 18h; Inert atmosphere; Sealed tube;

Reference yield:

: 1457966-68-5
N-benzyl-2,6-dichloro-3-nitropyridin-4-amine

: 1457967-15-5
N⁴-benzyl-3-nitro-6-phenyl-N²-(2,4,4-trimethylpentan-2-yl)-pyridine-2,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 48 h / Reflux

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate / water; 1,4-dioxane / 18 h / 90 °C / Inert atmosphere; Sealed tube

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; 2: |Suzuki Coupling;
DOI:10.1039/c3ob40816g