C₂₂H₃₂O₃

Base Information

Chemical Name:C₂₂H₃₂O₃
CAS No.:1412947-56-8
Molecular Formula:C₂₂H₃₂O₃
Molecular Weight:344.494
Hs Code.:

C<sub>22</sub>H<sub>32</sub>O<sub>3</sub>

Synonyms:C₂₂H₃₂O₃

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Chemical Property of C₂₂H₃₂O₃

Chemical Property:

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Technology Process of C₂₂H₃₂O₃

There total 8 articles about C₂₂H₃₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1412947-74-0
C₂₃H₃₆O₄

: 1412947-56-8
C₂₂H₃₂O₃

Guidance literature:: With sodium periodate; In water; tert-butyl alcohol; at 0 - 20 ℃;
DOI:10.1039/c2cc36260k

Reference yield:

: 88920-24-5
p-methoxybenzyloxy acetic acid

: 1412947-56-8
C₂₂H₃₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

4.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium iodide / butanone / 24 h / Reflux

6.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

6.2: 0 - 20 °C

7.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

8.1: sodium periodate / tert-butyl alcohol; water / 0 - 20 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; water; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; dichloromethane; water; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k

Reference yield:

: 65733-27-9
cis-piperitol

: 1412947-56-8
C₂₂H₃₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

4.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium iodide / butanone / 24 h / Reflux

6.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

6.2: 0 - 20 °C

7.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

8.1: sodium periodate / tert-butyl alcohol; water / 0 - 20 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; water; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; dichloromethane; water; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k