C₁₂H₁₄N₂O₃S

Base Information

Chemical Name:C₁₂H₁₄N₂O₃S
CAS No.:1314804-48-2
Molecular Formula:C₁₂H₁₄N₂O₃S
Molecular Weight:266.321
Hs Code.:

C<sub>12</sub>H<sub>14</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₁₂H₁₄N₂O₃S

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Chemical Property of C₁₂H₁₄N₂O₃S

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Technology Process of C₁₂H₁₄N₂O₃S

There total 2 articles about C₁₂H₁₄N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1314804-47-1
C₁₂H₁₂N₂O₃

: 1314804-48-2
C₁₂H₁₄N₂O₃S

Guidance literature:: With O,O-Diethyl hydrogen phosphorodithioate; In 1,4-dioxane; water; at 80 ℃; for 24h;
DOI:10.1016/j.bmcl.2011.05.006

Reference yield:

: 18595-18-1
3-amino-4-methyl benzoic acid methyl ester

: 1314804-48-2
C₁₂H₁₄N₂O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 5,5-dimethyl-1,3-cyclohexadiene / Reflux

2: O,O-Diethyl hydrogen phosphorodithioate / 1,4-dioxane; water / 24 h / 80 °C

With O,O-Diethyl hydrogen phosphorodithioate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; water;
DOI:10.1016/j.bmcl.2011.05.006

Reference yield:

: 1314804-48-2
C₁₂H₁₄N₂O₃S

: C₂₀H₁₅ClF₂N₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate

2.1: potassium carbonate / 20 °C

3.1: N-chloro-succinimide / isopropyl alcohol / 0.33 h / Reflux

3.2: 20 °C

With N-chloro-succinimide; sodium methylate; potassium carbonate; In isopropyl alcohol;
DOI:10.1016/j.bmcl.2011.05.006