N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide

Base Information

• Chemical Name: N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide
• CAS No.: 1204779-37-2
• Molecular Formula: C₅₀H₅₄N₂O₅
• Molecular Weight: 762.989
• Mol file: 1204779-37-2.mol

Synonyms:N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide

Chemical Property of N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide

There total 1 articles about N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

PDI-Si (1204779-43-0) → N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide (1204779-37-2)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1016/j.molstruc.2009.09.035

Reference yield: 58.0%

iodobenzene (591-50-4) + N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide (1204779-37-2) → N,N-dicyclohexyl-1-dodecyl-7-(4-ethynylbenzene)perylene-3,4,9,10-tetracarboxydiimide (1204779-40-7)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 50 ℃; for 1h;

DOI:10.1016/j.molstruc.2009.09.035

Reference yield:

N,N-dicyclohexyl-1-dodecyl-7-ethynyl-perylene-3,4,9,10-tetracarboxydiimide (1204779-37-2) + 1-iodo-4-(trimethylsilylethynyl)benzene (134856-58-9) → C61H66N2O5Si

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 50 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.molstruc.2009.09.035

upstream raw materials:

PDI-Si

Downstream raw materials:

N,N-dicyclohexyl-1-dodecyl-7-(4-ethynylbenzene)perylene-3,4,9,10-tetracarboxydiimide