(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate
CAS No.:1424362-24-2
Molecular Formula:C₁₇H₃₀N₂O₄S
Molecular Weight:358.502
Hs Code.:

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

Chemical Property:

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

There total 3 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1424362-19-5
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)acetate

: 1424362-24-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide; In tetrahydrofuran; at -45 ℃; for 1h;
DOI:10.1016/j.tetasy.2012.12.002

Reference yield:

: 921755-18-2
ethyl 2-(pentylsulfonyl)acetate

: 1424362-24-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / methanol / 3 h / 20 °C

2: dmap; benzoyl chloride; triethylamine / tetrahydrofuran / 6 h / 20 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide / tetrahydrofuran / 1 h / -45 °C

With dmap; benzoyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Methanesulfonyl azide; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2012.12.002

Reference yield:

: 2-(pentylsulfonyl)acetic acid

: 1424362-24-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-(pentylsulfonyl)diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; benzoyl chloride; triethylamine / tetrahydrofuran / 6 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; Methanesulfonyl azide / tetrahydrofuran / 1 h / -45 °C

With dmap; benzoyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Methanesulfonyl azide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2012.12.002