C₂₇H₃₀BrIO₂

Base Information

• Chemical Name: C₂₇H₃₀BrIO₂
• CAS No.: 1149765-46-7
• Molecular Formula: C₂₇H₃₀BrIO₂
• Molecular Weight: 593.342
• Mol file: 1149765-46-7.mol

Synonyms:C₂₇H₃₀BrIO₂

Chemical Property of C₂₇H₃₀BrIO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₀BrIO₂

There total 1 articles about C₂₇H₃₀BrIO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C27H31IO3 (1149765-45-6) → C27H30BrIO2 (1149765-46-7)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 25 ℃; for 2h; Inert atmosphere;

DOI:10.1002/chem.200802306

Reference yield: 92.0%

C27H30BrIO2 (1149765-46-7) + hydroquinone (123-31-9,8027-02-9) → C60H64I2O6 (1149765-47-8)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 72h; Inert atmosphere; Reflux;

DOI:10.1002/chem.200802306

Reference yield: 85.0%

C27H30BrIO2 (1149765-46-7) + C37H42O6 (1149765-55-8) → C64H71IO8 (1149765-53-6)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 12h; Inert atmosphere; Reflux;

DOI:10.1002/chem.200802306

upstream raw materials:

C₂₇H₃₁IO₃

Downstream raw materials:

C₆₄H₇₁IO₈

C₆₀H₆₄I₂O₆