C₂₉H₂₉FO

Base Information

• Chemical Name: C₂₉H₂₉FO
• CAS No.: 1313396-69-8
• Molecular Formula: C₂₉H₂₉FO
• Molecular Weight: 412.547
• Mol file: 1313396-69-8.mol

Synonyms:C₂₉H₂₉FO

Chemical Property of C₂₉H₂₉FO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₉FO

There total 4 articles about C₂₉H₂₉FO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

4-(2-(2,2-di-p-tolylvinylidene)-1-phenylcyclopropyl)butan-1-ol (1210959-95-7) → C29H29FO (1313396-69-8)

Guidance literature:

With Selectfluor; In acetonitrile; at 60 ℃; for 3h; Inert atmosphere;

DOI:10.1055/s-0030-1259715

Reference yield:

1,1-di(p-tolyl)ethylene (2919-20-2) → C29H29FO (1313396-69-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium tert-butylate / pentane

2.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / tetrahydrofuran / 36 h / 20 °C

3.1: diborane / tetrahydrofuran / 0 °C

3.2: 0 °C

4.1: Selectfluor / acetonitrile / 3 h / 60 °C / Inert atmosphere

With potassium tert-butylate; tetra(n-butyl)ammonium hydrogensulfate; Selectfluor; sodium hydroxide; diborane; In tetrahydrofuran; acetonitrile; pentane;

DOI:10.1055/s-0030-1259715

Reference yield:

1,1-dibromo-2,2-bis(4-methylphenyl)cyclopropane (70671-90-8) → C29H29FO (1313396-69-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / tetrahydrofuran / 36 h / 20 °C

2.1: diborane / tetrahydrofuran / 0 °C

2.2: 0 °C

3.1: Selectfluor / acetonitrile / 3 h / 60 °C / Inert atmosphere

With tetra(n-butyl)ammonium hydrogensulfate; Selectfluor; sodium hydroxide; diborane; In tetrahydrofuran; acetonitrile;

DOI:10.1055/s-0030-1259715

upstream raw materials:

1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-p-tolylvinyl)-4-methylbenzene

4-(2-(2,2-di-p-tolylvinylidene)-1-phenylcyclopropyl)butan-1-ol

1,1-di(p-tolyl)ethylene

1,1-dibromo-2,2-bis(4-methylphenyl)cyclopropane