methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside
CAS No.:688044-84-0
Molecular Formula:C₉₇H₁₀₇N₃O₂₅
Molecular Weight:1714.92
Hs Code.:

methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Synonyms:methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

There total 1 articles about methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 409060-32-8
2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

: 688044-83-9
methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: N-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)trichloroacetamide

: methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: 688044-84-0
methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; MS AW-300; In diethyl ether; at 20 ℃;
DOI:10.1002/ejoc.200300652

Reference yield: 89.0%

: 108-24-7
acetic anhydride

: 688044-84-0
methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[2-acetamide-6-O-acetyl-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: methyl (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-[6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->2)]-4,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptopyranoside; With hydrogen; Lindlar's catalyst; In ethyl acetate; for 72h;

acetic anhydride; In methanol; at 20 ℃; for 1h; Further stages.;
DOI:10.1002/ejoc.200300652