3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

Base Information

Chemical Name:3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate
CAS No.:1375313-74-8
Molecular Formula:C₃₄H₃₉N₅O₆S
Molecular Weight:645.78
Hs Code.:

Synonyms:3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

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Chemical Property of 3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

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Technology Process of 3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

There total 4 articles about 3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1375313-64-6
11-(1H-benzo[d][1,2,3]triazol-1-yloxy)-N-(4-hydroxy-1-methyl-2-oxo-1,2-dihydroquinolin-3-yl)undecanamide

: 98-59-9
p-toluenesulfonyl chloride

: 1375313-74-8
3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.ejmech.2012.03.003

Reference yield:

: 70744-03-5
3-amino-4-hydroxy-1-methyl-1H-quinolin-2-one

: 1375313-74-8
3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 12 h / 20 °C / Darkness

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.ejmech.2012.03.003

Reference yield:

: 36949-55-0
4-hydroxy-1-methyl-3-nitro-2-(1H)quinolinone

: 1375313-74-8
3-(11-(1H-benzo[d][1,2,3]triazol-1-yloxy)undecanamido)-1-methyl-2-oxo-1,2-dihydroquinolin-4-yl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 8 h / 20 °C

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / 12 h / 20 °C / Darkness

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.03.003