5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

Base Information

Chemical Name:5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid
CAS No.:77052-64-3
Molecular Formula:C₁₀H₇ClN₂O₃S₂
Molecular Weight:302.762
Hs Code.:

Synonyms:5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

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Technology Process of 5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

There total 2 articles about 5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 77052-41-6
5-(2-Chloro-phenoxymethyl)-3H-[1,3,4]oxadiazol-2-one

: 77052-64-3
5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

Guidance literature:: With ammonium hydroxide; for 2h; Ambient temperature;

Reference yield:

: [2-(2-Chloro-phenoxy)-acetyl]-urea

: 77052-64-3
5-(2-Chloro-phenoxymethyl)-2-oxo-[1,3,4]oxadiazole-3-carbodithioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / Br₂, NaOH / 0.25 h

2: 82 percent / NH₄OH / 2 h / Ambient temperature

With ammonium hydroxide; sodium hydroxide; bromine;