tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate

Base Information

• Chemical Name: tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate
• CAS No.: 231298-24-1
• Molecular Formula: C₂₀H₂₄N₂O₅
• Molecular Weight: 372.421

Synonyms:tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate

Chemical Property of tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate

There total 2 articles about tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

4-bromo-2-methylbut-1-ene (20038-12-4) + tert-butyl N-<2-(5-p-nitrophenylfuryl)>carbamate (226710-79-8) → tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate (231298-24-1)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In benzene; for 12h; Heating;

DOI:10.1021/jo982061+

Reference yield:

5-(4-nitrophenyl)-furan-2-carboxylic acid (28123-73-1) → tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate (231298-24-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / diphenylphosphoryl azide, Et₃N / 16 h / Heating

2: 57 percent / NaOH, K₂CO₃, Bu₄NHSO₄ / benzene / 12 h / Heating

With sodium hydroxide; diphenylphosphoranyl azide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triethylamine; In benzene;

DOI:10.1021/jo982061+

Reference yield: 82.0%

tert-butyl N-<3-(2-methylbutenyl)>-N-<2-(5-p-nitrophenyl)furyl>carbamate (231298-24-1) → 5-hydroxy-3a-methyl-5-p-nitrophenyl-3,3a,4,5-tetrahydro-2H-indole

Guidance literature:

In benzene; at 180 ℃; for 16h;

DOI:10.1021/jo982061+

upstream raw materials:

4-bromo-2-methylbut-1-ene

tert-butyl N-<2-(5-p-nitrophenylfuryl)>carbamate

5-(4-nitrophenyl)-furan-2-carboxylic acid

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